Glass reaction distillation integrated machine
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Glass reaction distillation integrated machine
- Product Details
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• New & Improved Open Frame Design Provides Excellent Accessibility
• Support Frame with Oversized Rugged S.S. Uprights and Heavy Duty PTFE Coated Aluminum Fittings
• Improved Support Clamp Auto-Centers Reactor and Lid Allowing Quick Installation/Removal Of Reactor
• Perfluoro O-Rings On 60mm and 200mm Flanges
• S.S. Inlet/Outlet Adapters Available In M16 x 1 and M30 x 1.5 Allow Connection To Cooling/Heating Circulator
• Lower Support Plate, and PTFE Ring, Have a "V" Shaped Opening Allowing An Unobstructed View Of Bottom Valve
• Zero Dead Space Detachable Drain Valve Has Knob with Laser Etched Directional Arrows For Open and Close
• Electric or Air Motor. Optional XP Motor Available
• 5-Neck Lid with Large Powder Addition Funnel
• Digital Temperature Monitor
• Electric Motor Has Separate Digital Controller
• Reactor Jacket Graduated On Both Sides
• Removable S.S. Pipe Used To Support Side Shelf and Manifold System
• Support Bushings For Optional Safety Shield
• Heavy Duty Lockable CastersProduct features and advantages:
1. According to the design concept of industrial reaction system, the product has added distillation function on the basis of single reaction synthesis, it can make distillation after the reaction, and remove low-boiling substances in the material, such as solvent, water, etc.;
2. The condenser adopts an abdominal wall vertical condenser, which increases the heat exchange area, and adds a low-temperature jacket to keep the cold outside, which increases the processing capacity during the distillation process and reduces the energy loss caused by the environmental impact on the equipment.
3. The product collection tank is added, which is convenient to operate. After the reaction is completed, open the bottom valve and discharge the material.
4. The product is designed with a liquid phase reflux distributor, which is switched by valve operation. If closing the valve to make reaction, the low-boiling point solvent or catalyst is heated, volatilized and then returned to the reaction kettle through cold trap cooling. If opening the valve to make distillation, the low boiler evaporates after being heated, and the steam enters the collection tank through the reflux distributor after condensing
5. The collection tank is connected to the return distributor with the method of the broadened mouth connection. The pipeline is made of PFA material, which has better anti-corrosion performance and intuitive observation. This design replaces hard connections of glass to reduces the risks of glass instruments’ damages during use or disassembly.
6. The solid feeding is changed to a screw cap design, which is convenient to open/close. The material is made of PTFE, and a sealing ring is added to the sealing part connected to the reaction kettle to improve the air tightness of the system;
7. The volume of the dripping tank is increased, which improves the processing capacity of the whole device;
8. The on-site pressure gauge display is added to the reaction kettle to ensure real-time observation of pressure changes during the reaction/distillation process to prevent the pressure from being held back in the reaction kettle. The pressure gauge is selected from high-precision products with an accuracy level of 1.0;
9. All valves are made of PTFE material, which has better sealing performance and is more convenient to clean/replace;
10. The mechanical stirring seal adopts a new design, which has better air tightness and is more stable during high-speed operation;
Parameter
Model A-GR-10-S A-GR-20-S A-GR-30-S A-GR-50-S A-GR-100-S The volume of the jacket of the kettle body L 3 6 8 16 30 Effective volume L 10 20 30 50 100 Condenser size (㎡) 0.25 0.35 0.45 0.6 0.95 Dropping tank volume L (mL) 1000 2000 2000 2000 10000 The size of the opening of the kettle lid Agitator Insert DN50 flange DN50 flange DN50 flange 50#Flange 60#Flange Temperature Sensor 34#Standard Grinding 34#Standard Grinding 34#Standard Grinding 34#Standard Grinding 34#Standard Grinding Condenser port DN50 Standard Grinding DN50 Standard Grinding DN50 Standard Grinding DN50 ball mill mouth DN50 ball mill mouth Liquid feed port 34#Standard Grinding 34#Standard Grinding 34#Standard Grinding 34#Standard Grinding 34#Standard Grinding Dropping tank connection DN40 Standard Grinding DN40 Standard Grinding DN40 Standard Grinding DN40 Standard Grinding DN40 Standard Grinding solid feed port DN80 flange cover DN80 flange cover DN80 flange cover DN80 flange cover DN80 flange cover Glass Components Borosilicate glass 3.3 Borosilicate glass 3.3 Borosilicate glass 3.3 Borosilicate glass 3.3 Borosilicate glass 3.3 Main frame SUS304 SUS304 SUS304 SUS304 SUS304 Paddle (option) Anchor/Paddle Anchor/Paddle Anchor/Paddle Anchor/Paddle Anchor/Paddle Motor Brushless DC Motor Brushless DC Motor Brushless DC Motor Brushless DC Motor Brushless DC Motor Move method Brake moving wheel Brake moving wheel Brake moving wheel Brake moving wheel Brake moving wheel Working temperature (℃) -80～200 -80～200 -80～200 -80～200 -80～200 Maximum temperature difference (℃) ≤80 ≤80 ≤80 ≤80 ≤80 The pressure in the kettle (bar) -1~0 -1~0 -1~0 -1~0 -1~0 Jacket pressure (bar) ≤0.3 ≤0.3 ≤0.3 ≤0.3 ≤0.3 Vacuum system boost rate (KPa/h) ≤2KPa/h ≤2KPa/h ≤2KPa/h ≤2KPa/h ≤2KPa/h Agitator motor power 120 120 120 180 200 Speed mode Frequency control Electronic Speed Control Electronic Speed Control Electronic Speed Control Electronic Speed Control Speed adjustment range 50～500rpm 50～500rpm 50～500rpm 50～500rpm 50～500rpm Temperature sensor PT100 PT100 PT100 PT100 PT100 Temperature measurement range -30~350℃ -30~350℃ -30~350℃ -30~350℃ -30~350℃ Interface size of stainless steel insulated hose 3/4 thread 3/4 thread 3/4 thread 3/4 male thread 3/4 male thread Sealing material PTFE PTFE PTFE PTFE PTFE Discharge valve installation height 320mm 320mm 320mm 320mm 380mm Power 220/240V
50/60Hz220/240V
50/60Hz220/240V
50/60Hz220/240V
50/60Hz220/240V
50/60HzAmbient temperature (℃) 5～35 5～35 5～35 5～35 5～35 Ambient relative humidity 65% 65% 65% 65% 65% Size (W×D×H mm) 840×640×1780 840×640×1910 840×640×1910 900×690×2100 1270×810×2400 Weight (kg) 48 67 75 82 119 Product Appearance Display
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