Product Category
Laboratory High Melting Point Distillation Unit & Continuous Wiped Film Distillation Unit
Product Description
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Product Introduction
In the process of rectification experiments, R&D personnel often encounter some products with high melting point and poor fluidity, and some products are in a solid state at room temperature. A high and low temperature cycle unit is used, but crystallization will occur at the return/extraction position, the connection of the discharge port, the vacuum airflow duct, the component outflow duct, the sampling position, and the component collection tank, which will affect the normal flow of materials and make the experiment. cannot be done. Generally, R&D personnel use glass wool heating tapes around the parts that are easy to crystallize to ensure that the experiment can continue, but this method brings many problems. Overheating phenomenon; if flammable and explosive liquid drips on the surface of the electric heating belt, it will bring safety hazards; the whole equipment is wrapped around the electric heating belt, which is not beautiful and will affect the observation during the experiment, so in order to solve these problems, I The company has developed a distillation system for high melting point substances.
During the research and development process of our company's R&D personnel, the original batch distillation unit components have been improved, so that the whole system has the function of heating and heat preservation. They are all connected in series, and heating and heat preservation is carried out by adding a thermal circulation oil bath or a high and low temperature unit. The reflux ratio part has also been improved. The technicians re-developed the reflux ratio. The new reflux ratio has the function of heating and heat preservation, and the reflux ratio adjustment is stable, which can realize long-term continuous work. Through the above research and development improvements, the product no longer crystallizes. , making the whole experiment simple and easy.
The high melting point substance rectification experimental device consists of a tower kettle, a magnetic stirring system, a thermal insulation condenser, a thermal insulation reflux ratio distributor, an electric heat tracing thermal insulation rectification tower, a packing, a thermal insulation vacuum sampler, a thermal insulation receiving tank, a cold trap, a thermal insulation vacuum Buffer tank, high and low temperature circulating oil bath unit, vacuum system, control system and other main components, all thermal insulation equipment are all designed with outer jacket, supporting external heating system to heat the jacket, supporting pipelines and valves are Jacketed design.
The glass high melting point rectification device is equipped with various specifications and models, which can be selected and matched for different product refining needs. All glass instrument connection parts are connected by thermal insulation flange ball mouth, which is very convenient for installation and replacement; the whole device is equipped with a temperature console, The reflux ratio console is used to control and adjust the temperature and the reflux ratio. The frame is designed with an integrated movable frame made of aluminum profiles, which is not only beautiful, but also easy to disassemble and install.
Technical parameter:
Batch/continuous designs available upon customer request
Equipment material: high borosilicate glass 3.3, stainless steel 316L, titanium alloy, Hastelloy, etc.
Tower diameter: DN32, DN40, DN50, DN80, DN100, etc. The specific specifications are subject to the process calculation results;
Tower height: There are four specifications of glass rectification tower, such as 500mm, 700mm, 1000mm, 1300mm, etc., which can be combined arbitrarily according to the requirements of the theoretical plate, or can be customized according to the physical properties and separation requirements after ASPEN calculation; packing: φ3mm/4mm /5mmθ ring wire mesh packing, glass spring packing, tetrafluoro Pall ring, structured packing, etc.
Tower kettle design temperature: normal temperature ~ 200 ℃ (high borosilicate glass), normal temperature ~ 300 ℃ (stainless steel)
Design pressure: -1bar～+0.5bar (high borosilicate glass), -1bar～5bar (stainless steel).
Return mode: liquid level difference return/forced return, the liquid level difference return is controlled by the return ratio distributor (ASK patented product), and the return ratio adjustment range is 1:99/99:1; it can also be controlled by a return tank + pump to achieve Reflux ratio adjustment.
Control system: PLC integrated control to realize temperature, pressure, reflux ratio, flow, liquid level, stirring speed control and real-time data acquisition.
Optional:
Vacuum system, heating cycle unit, refrigeration cycle unit, high and low temperature integrated machine: domestic/imported for customers to choose.
The above parameters are for reference only, and the specific technical requirements are customized according to customer needs.
Parameter specification table of glass/stainless steel intermittent device:
|
Effective volume of tower kettle（L） |
Main port connection specification |
Effective volume of receiving tank（L） |
Magnetic stirring device |
|
3 |
25ball flange connection |
1、1、2 |
ASK-A-8 |
|
5 |
40ball flange connection |
2、2、3 |
ASK-A-8 |
|
10 |
40ball flange connection |
2、2、10 |
|
|
20 |
40ball flange connection |
5、5、15 |
ASK-B-12 |
|
30 |
70ball flange connection |
10、10、20 |
|
|
50 |
70ball flange connection |
15、15、30 |
ASK-B-14 |
|
100 |
70ball flange connection |
30、30、50 |
ASK-B-14 |
Key words:
Order Process
Interesting
lnquiry
Inform usage scenarios and technical requirements
Recommended solution
Confirm the details, modify the plan
Customer confirm
Finished product testing, lssue running video and test report
Customer confirm
Production
Pay proofing fee
Recommended solution
Make Sample PI
Packing and shipping
Customer receipt
Guided installation and operation
Satisfied to Sign
Confirm bulk order
Products Can Be Custmized
The volume of the reactor has a wide selection range and can be customized according to customer needs;
The material of the equipment can be customized according to customer requirements, and can provide 304, 316, 316L, titanium alloy, Hastelloy, fluorine lining and other materials for selection.
Company Profile
Aishengke (Jiangsu) Chemical Technology Co., Ltd. was established in 2015. It is an engineering company specializing in providing small-scale research and development, pilot-scale scale-up, electronic-grade materials and fine chemicals industrialization equipment for reaction and separation operations. The company's address is located at No. 109, Liuyanghe Road, Xinbei District, Changzhou, Jiangsu Province. It has an office building of 1500 square meters, a R&D and analysis laboratory of 500 square meters, and an equipment processing and manufacturing plant of 4500 square meters.The company has a senior design team and a processing and manufacturing team, including process development, equipment design, 3D modeling and other designers, glass and stainless steel equipment processing and manufacturing groups, to ensure the high level of process technology development, simulation calculation, mechanical design and manufacturing process.
Why Choose Us
QUALITY
Quality frst is our basic philosophy.
TRANSPORT
Keep strong transportation capacity and excellent price.
WARRANTY
Warranty, parts and labor services.
PROJECT TEAM
A complete project team to provide customers with one-stop service.
Our Certificate
After-sales Service
Replace damaged parts
One year warranty lifetime maintenance
Online technical support
Process
Shot the acceptance video
Submit video within 7 days with broken or missing parts
Reissue parts by express
Faq
Yes, we can provide samples. Considering the high value of our products, samples are not free, but we will give you the best price.
We Have Our Own Factory. We Are Experts In Reaction And Separation Process Technology. With Wanhua, Huawei, Smic And Many Other Customers, It Has Won Wide Acclaim In The Industry.
rotary evaporator, alcohol recovery equipment, short path distillation kit, glass molecular distillation equipment, falling film evaporator, jacketed glass reactor and other lab equipment.
Generally it is within 7 working days after receiving the payment if the goods are in stock. Or it is 15 working days if the goods are not in stock, depending on order quantity.
Payment≤15,000USD, 100% in advance. Payment≥15,000USD, 70% T/T in advance, balance before shipment. (If you are concerned about payment security for the first order, we advise you can place Trade Assurance Order via Alibaba. you will get 100% payment refund if we can't meet agreed delivery time.)
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If you recognize the brand, technology, products and market prospects of Aishengke, we look forward to establishing a strategic partnership with you for win-win cooperation and development. Looking forward to your joining!
Contact Us
Manager Han: +86 150 5197 5149
Landline: +86 0519-85611172
Fax: +86 0519-85611132
Address: 3rd Floor, Office Area, No. 109, Liuyanghe Road, Xinbei District, Changzhou City